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dc.contributor.authorBaldin, Estela Knopp Kerstnerpt_BR
dc.contributor.authorMalfatti, Célia de Fragapt_BR
dc.contributor.authorRodói, Vanessapt_BR
dc.contributor.authorBrandalise, Rosmary Nichelept_BR
dc.date.accessioned2020-01-16T04:09:13Zpt_BR
dc.date.issued2019pt_BR
dc.identifier.issn1687-8434pt_BR
dc.identifier.urihttp://hdl.handle.net/10183/204349pt_BR
dc.description.abstractThe objective of this study was to evaluate the influence of sterilization on a hybrid coating obtained from a sol composed of alkoxysilane tetraethoxysilane (TEOS) and organoalkoxysilane methyltriethoxysilane (MTES) containing 10% (mass) of hydroxyapatite particles. The coating was obtained by dip coating, by applying two layers (protective/bioactive), which were cured at different temperatures (450°C and 60°C). The effects of sterilization on the superficial, electrochemical, bioactive, and mechanical properties of the coating were evaluated by performing different sterilization processes, namely, steam autoclave, hydrogen peroxide plasma, and ethylene oxide. Subsequently, the coating was characterized by using scanning electron microscopy (SEM/ FEG), and FTIR measurements were performed to characterize the chemical structure. The bioactivity and degradability of the coating were analyzed by mass variation after immersion in SBF and X-ray diffraction (XRD) analysis. )e electrochemical behavior was assessed by open circuit potential (OCP) and potentiodynamic polarization curves and the mechanical behavior by wear resistance. Results showed that all sterilization processes caused significant morphological changes in the hybrid coating. The autoclaved sample presented the highest structural chemical changes, and, consequently, the highest degradability, even though it had a superior bioactive behavior in relation to the other samples. In addition, the sterilization processes influenced the electrochemical behavior of the hybrid coating and altered the mechanical resistance to abrasion, thus presenting lower wear performance in relation to the nonsterilized sample.en
dc.format.mimetypeapplication/pdfpt_BR
dc.language.isoengpt_BR
dc.relation.ispartofAdvances in materials science and engineering. New York. Vol. 2019 (2019), 8593193, 13 p.pt_BR
dc.rightsOpen Accessen
dc.subjectRevestimentopt_BR
dc.subjectHidroxiapatitapt_BR
dc.subjectEsterilizaçãopt_BR
dc.titleEffect of sterilization on the properties of a bioactive hybrid coating containing hydroxyapatitept_BR
dc.typeArtigo de periódicopt_BR
dc.identifier.nrb001107261pt_BR
dc.type.originEstrangeiropt_BR


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